Academia

Rapid-access Synchrotron X-ray Scattering for Research Groups

Publication-ready synchrotron data. No proposal. No travel. No beamline expertise required. We provide high-resolution powder diffraction, pair distribution function analysis, and small-angle scattering data with a two-week turnaround and academic-friendly pricing.

Three complementary techniques. One workflow.

PXRD

Phase identification and quantification, crystal structures, microstructure, defects. Improved detection with ~200× better signal-to-noise than lab XRD

Total Scattering / PDF

Local atomic structure of amorphous, nanocrystalline, and disordered phases — bond lengths, coordination environments, cluster sizes — no long-range order required

SAXS

Microstructural properties on the scale of 1–100 nm, e.g., particle size distributions, porosity, and phase distribution

Why use a measurement service instead of writing a proposal?

The traditional route to synchrotron beamtime — proposal writing, submission, peer review, competitive allocation, travel to the facility, on-site operation of complex instrumentation — was designed for frontier research and has served that purpose well. But it was not designed for the researcher who needs routine characterisation of large sets of samples or who needs results on a predictable timeline to inform the next experiment.

We fix the access problem.

Get synchrotron data in ~2 weeks, not 6–12 months. No proposal writing. No travel.

Ship your samples by international courier. We handle sample preparation, measurement at ESRF (ID31) and soon at DESY as well, data reduction, and delivery of publication-ready data through our online portal. The two-week turnaround means that your projects don’t have months of delay waiting for beamtime allocation.

No data processing burden.

You focus on the science. We focus on the data. All raw data are automatically processed with appropriate calibration, geometric and detector-specific corrections, background subtraction, and validation against NIST standards. For PDF, data normalisation and transformation using PDFgetX3 are performed as part of the standard service. Instrumental profile effects are determined for software including TOPAS, GSAS-II, PDFgui, and Diffpy-CMI. You receive analysis-ready data for Rietveld or real-space refinement, together with instrumental resolution functions and starter files.

Scale effortlessly from 5 to 500 samples using the same workflow.

Whether you need a quick phase identification on a few samples or a comprehensive study across an entire parameter space, the process and quality remain identical. No minimum batch requirements. No upper limit on throughput.

Resolution and sensitivity that changes what you can see.

With instrumental resolution of ΔQ/Q < 3·10⁻³ at Q ≈ 1.5 Å⁻¹ — approximately 2–5 times better than a typical Bragg–Brentano diffractometer — you resolve overlapping peaks, detect trace phases down to 0.1–0.01 wt%, and obtain structural detail inaccessible with lab instruments. Groups accustomed to laboratory data routinely discover that features they had attributed to the sample are in fact instrumental artefacts — and conversely, that structural detail of genuine scientific interest becomes accessible for the first time.

The FAIR Data Plan

Academic researchers access the service through our FAIR Data Plan — discounted pricing per measurement, inclusive of sample preparation, data reduction, and an experimental report.

How it works:

  • Measurement data are held under a 24-month embargo to protect your publication priority
  • After 24 months, data become available as an open resource through the MatScatNet initiative, funded through the OSCARS programme
  • This aligns with FAIR data principles (Findable, Accessible, Interoperable, Reusable) and the digital infrastructure policies of the European Commission
  • Credits are valid for 12 months and can be applied flexibly across any scheduled beamtime

What you contribute to:

a growing, curated reference library of high-quality synchrotron powder diffraction and total scattering data — an open resource that benefits the entire research community and enables the development of machine learning methods for structural analysis.

What you get:

synchrotron-quality data at a fraction of the cost of proprietary measurements, with the same data quality, turnaround, and service level.

What does this mean for your research?

Phase identification & quantification (PXRD):

Resolve phases that overlap on lab instruments. Detect trace phases and impurities that sit below lab detection limits. Obtain accurate quantification of components for multiphase mixtures.

Structure solution (PXRD):

Data quality suitable for structure solution of microcrystalline materials from powder diffraction with high reciprocal space resolution for accurate partitioning of intensities and good structural resolution down to approx. 0.69 Å in high-resolution mode.

Local structure & amorphous materials (PDF):

Probe the structure of materials that lack long-range order. Characterize amorphous precursors, nanocrystalline products, disordered intermediates, glassy phases, or ultra-small clusters. Differential PDF isolates the structural contribution of deposited or intercalated species from their host matrix.

Microstructure & mesoscale organisation (SAXS):

Characterize particle size distributions, pore structures, and phase distribution in nanoparticles, framework materials, colloidal systems, or composite architectures.

High-throughput screening & combinatorial studies:

Map phase formation across large parameter spaces including precursor species, synthesis temperature, solution pH, dopant concentration, etc. Statistical analysis, clustering, and compositional mapping across hundreds or thousands of samples — at a throughput no lab instrument can achieve.

Reproducibility & long-term comparability:

Reference standards (NIST LaB₆ SRM 660b, CeO₂, Si SRM 640c) are measured alongside every user batch. Refined lattice parameters demonstrate reproducibility across sessions separated by months. This is not one-off beamtime data — it is a calibrated, traceable measurement service.

Use Cases

New material characterisation
Verification of crystallinity and novelty, identification of structure types, quantification of side phases.
Structure solution from powders
High-resolution data suitable for ab initio structure determination.
Systematic composition studies
Map phase boundaries, solid-solution limits, or dopant incorporation across a parameter space.
Amorphous & disordered materials
Local structure characterisation of glasses, gels, amorphous precursors, or nanocrystalline phases.
Nanoparticle & cluster analysis
Bond lengths, coordination environments, domain size, and internal structure of nanoscale systems.
Framework materials (MOFs, COFs, zeolites)
Phase purity, crystallinity, pore structure, and guest loading.
Energy materials (batteries, thermoelectrics, electrocatalysts)
Phase evolution, degradation products, solid-solution mapping, defect characterisation.
High-throughput / combinatorial screening
Statistical clustering and compositional mapping across large sample libraries.
ML/AI training datasets
High-quality, standardised diffraction patterns with consistent geometry and minimal artefacts — enriched and labeled data for training machine learning models.

How it works

1

Register

Create an account on the Momentum Transfer data portal. Submit a measurement request.

2

Ship

Mail your samples by international courier. No special preparation needed for standard powders.

3

Measure

Synchrotron PXRD/PDF/SAXS on high-throughput beamlines at ESRF (ID31).

1–2 weeks

4

Results

Publication-ready data delivered through the online portal. Calibrated, background-corrected, with resolution functions and refinement starter files.

within days after measurement

Optional add-ons: Rietveld refinement, PDF analysis, SAXS model fitting, statistical analysis, custom reporting.

Data Analysis

Measurement only

What You Get

Raw and processed data, experimental report

Best For

Groups with in-house analysis expertise, ML/AI training datasets

Semi-quantitative (Rietveld)

What You Get

Full phase ID + relative wt%

Best For

Multiphase systems, synthesis and process optimisation

Full quantitative (Rietveld + internal calibrant)

What You Get

Full phase ID + absolute quantification incl. amorphous content

Best For

Mining and minerals; geological studies and waste materials

Statistical & cluster analysis

What You Get

Clustering, compositional mapping

Best For

Combinatorial studies, high-throughput screening

PDF / local structure analysis

What You Get

Pair distribution function for amorphous, nanocrystalline, and disordered phases

Best For

Nanomaterials, glasses, disordered systems, catalysts

SAXS

What You Get

Microstructure: phase distribution, particle size, porosity

Best For

Nanoparticles, porous frameworks, colloids, soft matter

Sample Requirements

Sample mass
30–50 mg (standard)
Crystallite size
Ideal range < 1–5 µm. Milled & homogenised powders are best.
Accepted forms
Powders, gels, foams, slurries, suspensions, solutions. Polycrystalline solids such as pellets, discs, or films also work (assuming grain sizes as above).
Air/moisture-sensitive
Sealed vials or inert-packed holders accepted
Shipping
Use a certified international courier only (DHL, FedEx, UPS, etc.)
Sample storage
Retained for 3 months and then destroyed. Let us know if you need samples returned.

Technical Infrastructure

Facilities
ESRF (ID31, Grenoble) + DESY (Hamburg planned)
X-ray energy
75.0 keV (λ ≈ 0.165 Å)
Detector
Pilatus4 X CdTe 4M — large-area, hybrid photon-counting detector, zero readout noise, high dynamic range, high quantum efficiency at 75 keV
Resolution
ΔQ/Q > 3·10⁻³ at Q ≈ 1.5 Å⁻¹ (2–5× finer than typical lab device)
Geometry
Flat-plate transmission — thick probe volume; powder fluidisation minimises preferred orientation
Throughput
1 000+ samples per shift. No lab instrument approaches this by any margin.
Calibration
NIST LaB₆ SRM 660b, verified with 674b (ZnO, TiO₂, CeO₂) and Si SRM 640c every session
PDF reduction
PDFgetX3. S(Q), F(Q), and G(r) provided with reprocessing possibilities.

Publication Track Record

In 2025 alone, data collected in less than 3 days of total beamtime through the service contributed to over 50 peer-reviewed publications in journals including:

Nature Nanotechnology · Advanced Materials · Advanced Functional Materials · Nano Energy · Angewandte Chemie · Journal of the American Chemical Society · Nature Communications · Advanced Science · Science Advances · ACS Applied Materials & Interfaces

Research topics span energy storage · thermoelectrics · heterogeneous catalysis · functional ceramics · porous framework materials · high-pressure physics · nanomaterials · pharmaceutical formulations · polymers · metallurgy. A maintained publication list is available at momentum-transfer.com/publications.

The Numbers

1 000+ worldwide

Registered researchers

800+

Customer requests (2025)

8 000+

Individual measurements (2025)

50+

Peer-reviewed publications (2025)

ESRF + DESY (planned)

Synchrotron facilities

Multiple per month

Beamtime sessions

Why this costs less than you think

A laboratory diffractometer costs €250 000+ in capital, plus maintenance, staffing, consumables, and lab space. For a research group requiring high quality data on hundreds of samples per year, the FAIR Data Plan provides synchrotron-quality data — data that surpass what any laboratory instrument can deliver — for a fraction of that cost. No CAPEX. No maintenance. No expert team on your side required.

For groups that need occasional access to high-resolution capabilities, the economics are particularly compelling. You pay for measurements and analysis, not infrastructure.

Multimodal characterisation is becoming more important for advanced materials and frustrated structures. Our service provides access to pair distribution function and small-angle scattering characterisation, often not available in laboratory settings, to complement your analysis over a wide range (approx. 100–0.1 nm) of length-scales.

Let our expert team complement your lab. We can provide advanced analysis capabilities to newcomers, and help onboard your research team to these tools and techniques.

Founded by researchers. Built for researchers.

Momentum Transfer was founded by materials scientists from BASF and the Max Planck Institute for Solid State Research. The company completed its spin-out from BASF's Chemovator incubator in mid-2025 and is headquartered at the DESY Start-up Labs Hamburg. Operations at ESRF continue through a partnership providing regularly scheduled beamtime on ID31. The MEDESES project (BMBF, ErUM-Transfer, 05K24XUA) — a collaboration between DESY, ESRF, and Momentum Transfer — is building identical measurement capability at DESY's P25 beamline, creating a dual-facility platform with cross-comparable data.

Ready to get synchrotron data for your research?

Book a free 30-minute consultation. Discuss your samples, your scientific questions, and which combination of methods makes sense.